Determination of 30 Per- and Polyfluoroalkyl Substances in Dry Soybeans

Agilent Captiva EMR PFAS Food cartridges were developed and optimized specifically for per- and polyfluoroalkyl substance (PFAS) analysis in food. The objective of this study was to develop and validate a complete workflow for the determination of 30 PFAS in dry soybeans. The method uses QuEChERS extraction followed by enhanced matrix removal (EMR) mixed-mode passthrough cleanup using a Captiva EMR PFAS Food II cartridge and detection with an Agilent 6495D triple quadrupole LC/MS (LC/TQ). The method was validated to meet AOAC Standard Method Performance Requirements (SMPR) 2023.003 , including method suitability, sensitivity, accuracy, and precision.

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